Chapter 1 Tip-Enhanced Raman Spectroscopy 1
1.1 Introduction 1
1.2 A novel technique: TERS 3
1.2.1 Diffraction limit 3
1.2.2 TERS mechanisms 5
1.. TERS setup 7
1.3 TERS samples and tips 13
1.3.1 Sample preparation 13
1.3.2 Tip preparation 14
1.4 References 16
Chapter 2 High-Vacuum Tip-Enhanced Raman Spectroscopy 25
2.1 Introduction 25
2.2 Description of the HV-TERS system 26
. Experimental validation of the HV-TERS system 32
2.4 Discussion 34
2.5 References 38
Chapter 3 Recent Advances Regarding TERS and HV-TERS 42
3.1 Introduction 42
3.2 Recent advances 43
3.2.1 Single-molecule detection and sub-molecule resolution 43
3.2.2 Plasmon-driven reactions 50
3.. In-situ local temperature 57
3.2.4 Nonlinear TERS 58
3.2.5 TERS for materials 63
3.2.6 Ultrafast tip-enhanced Raman spectroscopy 67
3.2.7 Deep ultraviolet (DUV) TERS 67
3.3 Summary and outlook 69
3.4 References 71
Chapter 4 Tip-Enhanced Fluorescence (Plasmon-Enhanced Fluorescence) 78
4.1 Introduction 78
4.2 The principle of PEF 79
4.3 PEF from various geometrical metallic plasmonic nano structures 81
4.3.1 Interaction of fluorophores with surface plasmons 81
4.3.2 PEF from periodical metallic plasmonic nanostructure 83
4.3.3 PEF from non-periodical metallic plasmonic nanostructure 90
4.4 The wavelength and spacer effect towards the fluorescence enhancement 95
4.5 The tip-enhanced effect towards the fluorescence emissions 97
4.6 PEF from rare-earth doped nanoparticle 102
4.7 Conclusion and outlook 105
4.8 References 105
Chapter 5 In-Situ Measurements of Tip-Enhanced Raman and Fluorescence Spectroscopy 115
5.1 Introduction 115
5.2 Theoretical analysis 116
5.3 Analysis methods 126
5.4 References 126
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Mengtao Sun obtained his Ph.D. in2003 from State Key Laboratory of Molecular Reac-tion Dynamics, Dalian Institute of Chemical Physics, Chinese Academy of Sciences(CAS). From 2003 to 2006, he worked as a postdoc at the Department of ChemicalPhysics, Lund University. Since 2006, as an Associate Professor, he has worked at theBeijing National Laboratory for Condensed Matter Physics, Institute of Physics, CAS.Since 2016, he is the full profess at Beijing Key Laboratory for Magneto-PhotoelectricalCoite and Interface Science, School of Mathematics and Physics, the University ofScience and Technology Beijing. His current research interests focus on Tip-enhancedRaman spectroscopy (TERS). Researcher : B-1131-2008. In 2016, he was honored theScience and Technology (Natural Science) Award of Liaoning Province (the second prize).
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