醉染图书逸出气体分析(第二版)9787566920027

章 逸出气体分析简介 Introduction to Evolved Gas Analysis(1)第2章 热重-质谱联用技术TGA-MS(6)2.1质谱的原理 Principles of MS(6)2.2TGA-MS 测量系统 The TGA-MS System(8).测量模式 Measurement Modes(9)2.4结果解释 Interpretation of Results(11)2.5典型的碎片化模式 Typical Fragmentation Patterns(15)2.6结果表述 Presentation of Results(16)第3章 热重-红外光谱联用技术TGA-FTIR (17)3.1FTIR的原理 Principles of FTIR(17)3.2TGA-FTIR系统 The TGA-FTIR System(21)3.3曲线表示 Presentation of Results(2).4解析方法 Interpretation Procedure(24)3.5光谱的解析 Interpretation of Spectra(26)3.6特征吸收频率 Characteristic Absorption Frequencies(27)3.7结果表述 Presentation of Results(29)第4章 热重分析-气相色谱/质谱联用技术TGA-GC/MS (30)4.1GC的原理 Principles of GC(30)4.2TGA-GC/MS系统 The TGA-GC/MS System(35)4.3测量可行 Measuremensibilities(36)4.4测量结果 Results(39)第5章 热重分析-微型气相色谱/质谱联用技术TGA-Micro GC/MS (41)5.1微型气相色谱仪的原理 Principles of Micro GC(41)5.2TGA-Micro GC和TGA-Micro GC/MS系统 TGA-Micro GC and TGA-Micro GC/MS Systems(44)5.3实验结果 Results(45)第6章 应用简介 Introduction to the Applications (46)第7章应用介绍 Applications List (49)7.1通过TGA-MS、TGA-FTIR和TGA-MicroGC研究一水合草酸钙的分解机理 Decoition of Calcium Oxalate Monohydrate (Tutorial) by TGA-MS, TGA-FTIR and TGA-Micro GC(55)7.2通过TGA-MS和TGA-FTIR研究五水合硫酸铜的分解机理 Decoition of Copper Sulfate Pentahydrate (Tutorial) by TGA-MS and TGA-FTIR(57)7.3实验条件对MS灵敏度的影响分析 Influence of Experimental Conditions on MS Sensitivity(59)7.4通过TGA-MS和TGA-GC/MS多次进样法研究乙酰水杨酸的分解Decoition of Acetylsalicylic Acid by TGA-MS and TGA-GC/MS Multi-injection(65)7.5通过TGA-FTIR研究BHET的热降解Thermal Degradation of BHET by TGA-FTIR(67)7.6通过TGA-FTIR研究工业月桂醇的分解Decoition of Technical Lauryl Alcohol by TGA-FTIR(70)7.7通过TGA-MS检测药物中的残留溶剂Detection of Residual Solvents in a Pharmaceutical Substance by TGA-MS(72)7.8通过TGA-MS研究填充有机物的沸石的解吸附Desorption of a Zeolite Filled with Organic Matter by TGA-MS(73)7.9通过TGA-MS研究PVC粉末的热裂解Pyrolysis of PVC Powder by TGA-MS(76)7.10通过TGA-FTIR研究氟化电缆线Investigation of Fluorinated Cable Wires by TGA-FTIR(78)7.11通过TGA-MS检测橡胶样品中的水杨酸甲酯Detection of Methyl Salicylate in a Rubber Sample by TGA-MS(80)7.12通过TGA-FTIR研究有机硅聚合物的降解Degradation of a Silicone Polymer by TGA-FTIR(81)7.13通过TGA-MS和TGA-FTIR研究氨基树脂的固化和分解 Curing and Decoition of an Amino Resin by TGA-MS and TGA-FTIR(83)7.14通过TGA-FTR和SC研究热转变和分解以鉴别BR和NR橡胶Identification of BR and NR Rubbers. Study of Thermal Transitions and Decoition by TGA-FTIR and DSC(85)7.15通过TMA-MS研究印刷电路板的分层Delamination of Printed Circuit Boards by TMA-MS(88)7.16通过TMA-MS研究用于封装发泡剂的聚合物的膨胀和分解Expansion and Decoition of a Polymer Used To Encapsulate a Blowing Agent by TMA-MS(89)7.17通过TGA-MS测定离子液体中的水分含量Determination of the Water Content of an Ionic Liquid by TGA-MS(91)7.18通过TGA-FTIR研究热裂解并阐明阻燃机理From the Investigation of Pyrolysis to the Elucidation of Fire Retardancy Mechanisms by TGA-FTIR(93)7.19通过TGA-MS和DSC研究高熔点陶瓷High Melting Ceramics by TGA-MS and DSC(97)7.20通过TGA-MS和显微DSC研究唑来膦酸水合物的热行为Thermal Behavior of Zoledronic Acid Hydrate by TGA-MS and DSC-Microscopy(100)7.21通过TGA-MS定量分析钴粉中的氧化钴ntification of Cobalt Oxide in a Coated Cobalt Powder by TGA-MS(103)7.22通过TGA-GC/MS和TGA-Micro GC/MS研究聚酰胺66的分解产物Investigation of Evolved Decoition Products of Polyamide66by TGA-GC/MS and TGA-Micro GC/MS(104)7.通过TGA-GC/MS、DSC和DMA鉴定多组分热塑树脂Identification of Multi-Component Thermoplastics by TGA-GC/MS, DSC and DMA(107)7.24通过TGA-GC/MS、DSC、DMA和ATR研究橡胶的变形原因Deformulation of a Rubber by TGA-GC/MS, DSC, DMA and ATR(113)7.25通过TGA-GC/MS-FTIR测定聚丙烯材料有无磷酸铵阻燃剂的质Polypropylene with and without Ammonium Phosphate Flame Retardant by TGA-GC/MS-FTIR(120)7.26通过TGA-GC/MS对EPDM橡胶进行热氧化研究Thermal Otion of EPDM Rubber by TGA-GC/MS(125)7.27通过TGA-MS和TGA-GC/MS定量分析涂料中的二甲基甲酰胺（DMF）ntification of Dimethylformamide in Coatings by TGA-MS and TGA-GC/MS(129)7.28TGA-GC/MS定量测定天然橡胶中低含量的丁苯橡胶ntification of a Low Content of Styrene-Butadiene Rubber in Natural Rubber by TGA-GC/MS(134)7.29通过TGA-Micro GC/MS技术分析酚醛树脂的分解产物Evolved Decoition Products of a Phenol-Formaldehyde Resin by TGA-Micro GC/MS(137)7.30通过TGA-Micro GC/MS技术定量分析焦炭样品中的二氧化碳ntification of Carbon Dioxide in a Coke Sample by TGA-Micro GC/MS(140)7.31TGA-Micro GC/MS、TMA和DSC用于钛酸钡的合成和表征Synthesis and Characterization of Barium Titanate by TGA-Micro GC/MS, TMA and DSC(142)7.32用TGA-Micro GC/MS和Karl Fischer滴定仪测定热塑塑料中的水含量Determination of Water Content in a Thermoplastic by TGA-Micro GC/MS and Karl Fischer titratr(47)7.33通过TGA-GC/MS和TGA-Micro GC/MS物质样品Study of a Biomass Sample by TGA-GC/MS and TGA-Micro GC/MS(151)7.34通过 TGA-GC/MS和TGA-Micro GC/MS分析由褐煤释放出的气体Gases Evolve fo Lignite by TGA-GC/MS and TGA-Micro GC/MS(157)参考书目 Literature(164)缩写和首字母缩写词 Abbreviations and Acronyms(165)