正版 有机化学实验(四川大学精品立项教材)(英文版) 编者:吴凯群|

Part 1 Introduction
1.1 Foreword to the student
1.2 General laboratory safety
1.2.1 Laboratory dress code
1.2.2 Essential rules for laboratorv safetv
1.2.3 Working safely and efficiently
1.2.4 Miscellaneous information
1.3 How to write a laboratory reDort
1.3.1 The pre-laboratory／experimental preview record
1.3.2 The in-laboratory record
1.3.3 The post-laboratory write-up
1.3.4 An example for a laboratory report
1.4 Disposal of laboratory waste
1.5 Laboratory equipment
Part 2 Basic Experimental Techniques
2.1 Technique 1：Distillation
2.1.1 Simple distillation
Experiment 1 Simple distillation and the determination of boiling point
2.1.2 Fractional distillation
Experiment 2 Separation of ethanol—water mixture with fractional distillation
2.1.3 Steam distillation
Experiment 3 Extraction of paeonolum from Xuchangqing
2.1.4 Vacuum distillation
2.1.5 Rotary evaporator
2.2 Technique 2：Reflux
2.2.1 Glassware／Equipment checklist
2.2.2 Utilizing the apparatus
2.3 Technique 3：Recrystallization
Experiment 4 Recrystallization of benzoic acid
2.4 Technique 4：Melting point determination
Experiment 5 Determination of melting point
2.5 Technique 5：Liquid-liquid extraction
2.5.1 Assemble a separatory funnel
2.5.2 Use a separatory funnel
2.5.3 Determine the nature of your layer
Experiment 6 Simple extraction and multiple extractions
2.6 Technique 6：Chromatographic techniques
2.6.1 Thin-layer chromatography
Experiment 7 Separation of green lear pigments by TLC
2.6.2 Column chromatography
Experiment 8 Separation of dyestuffs by column chromatography
2.6.3 Paper chromatography
Experiment 9 Separation of amino acid by paper chromatography
2.7 Technique 7：Sublimation
2.8 Technique 8：Measurement of refractive index
Experiment 10 Identify the substance by refractometry
2.9 Technique 9：Measurement of optical rotation
Experiment 1 1 Measure the optical rotation of a sample
Part 3 Basic Organic Synthesis Experiments
Experiment 12 Synthesis of cyclohexene
Experiment 13 Synthesis of p-toluidine
Experiment 14 Preparation of 1，4一Di—tert-2，5-dimethoxybenzene
Experiment 15 Nitration of methyl benzoate
Experiment 16 Preparation of n-butyl bromide
Experiment 17 Preparation of triphenylmethanol
Experiment 18 Preparation of trans-9一(2一phenylethenyl)anthracene
Experiment 19 Preparation of 2一furanmethanol and 2一furoic acid
Experiment 20 Synthesis of cinnamic acid
Experiment 21 Luche reduction of L-menthone
Experiment 22 Preparation of ethyl acetate
Experiment 23 Synthesis of propyl acetate
Experiment 24 Synthesis of aspirin(acetylsalicylic acid)
Experiment 25 Preparation of acetanilide
Experiment 26 Preparation of methvl orange
Experiment 27 Synthesis of 9，10-dihydroanthracene-9，10-endo-α，β-succinic anhydride
Part 4 Reaction of Natural Products
Experiment 28 Isolation of effective components from the citrus
Experiment 29 Isolation of caffeine from tea
Experiment 30 Isolation of benberine from Coptis fhinensis Franch
Experiment 31 Preparation of soap
Part 5 Property Experiments of Organic Compounds
5.1 Qualities test for the element
5.1.1 Principle
5.1.2 Method
5.2 Test for the functional group
Appendix
Appendix I Common organic solvents
Appendix II List of the elements with their symbols and atomic masses

吴凯群，四川大学化学学院副教授，理学博士。从事有机化学理论课和实验教学二十余年，近年来参与了《基础有机化学》和《有机化学实验》的编写工作。

本书是根据国内实际情况，在总结多年来有机化学实验的教学经验及近年来实施全英文教学实践的基础上编写的与有机化学全英文课程配套使用的教材。全书共五章，内容包括有机化学实验的基本知识、有机化学实验基本操作和技术以及有机化合物的分离提纯方法与技术、基本有机合成实验、天然产物的提取和分离、一些元素和官能团的性质实验等。本教材可使学生在掌握有机化学实验基本原理、基本技能的同时提高英语实际应用能力和水平，适用于化学、医学、药学、生命科学及相关专业的学生。